1-(Benzyloxy)-2-methoxy-4-(2-nitroprop-1-en-1-yl)benzene

Base Information

Chemical Name:1-(Benzyloxy)-2-methoxy-4-(2-nitroprop-1-en-1-yl)benzene
CAS No.:321125-48-8
Molecular Formula:C17H17 N O4
Molecular Weight:299.326
Hs Code.:2909309090
DSSTox Substance ID:DTXSID40697973
Mol file:321125-48-8.mol

Synonyms:DTXSID40697973;WNVPWPSALZVHTN-UHFFFAOYSA-N;MFCD02258792;SY294220;1-(4-benzyloxy-3-methoxy-phenyl)-2-nitropropene;1-benzyloxy-2-methoxy-4-(2-nitropropenyl)benzene;1-benzyloxy-2-methoxy-4-[2-nitroprop-1-enyl]benzene;(E)-1-(Benzyloxy)-2-methoxy-4-(2-nitro-1-propenyl)benzene;1-(Benzyloxy)-2-methoxy-4-(2-nitroprop-1-en-1-yl)benzene

Suppliers and Price of 1-(Benzyloxy)-2-methoxy-4-(2-nitroprop-1-en-1-yl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(4-BENZYLOXY-3-METHOXYPHENYL)-2-NITROPROPENE 95.00%
5MG
$ 505.05

Total 3 raw suppliers

Chemical Property of 1-(Benzyloxy)-2-methoxy-4-(2-nitroprop-1-en-1-yl)benzene

Chemical Property:

Melting Point:89-90 °C
Boiling Point:454.9±35.0 °C(Predicted)
PSA：64.28000
Density:1.189±0.06 g/cm3(Predicted)
LogP:4.43490
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:299.11575802
Heavy Atom Count:22
Complexity:385

Purity/Quality:

98% ^*data from raw suppliers

1-(4-BENZYLOXY-3-METHOXYPHENYL)-2-NITROPROPENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC1=CC(=C(C=C1)OCC2=CC=CC=C2)OC)[N+](=O)[O-]

Technology Process of 1-(Benzyloxy)-2-methoxy-4-(2-nitroprop-1-en-1-yl)benzene

There total 3 articles about 1-(Benzyloxy)-2-methoxy-4-(2-nitroprop-1-en-1-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 79-24-3
Nitroethane

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 321125-48-8
1-benzyloxy-2-methoxy-4-[2-nitroprop-1-enyl]benzene

Guidance literature:: With ammonium acetate; for 17h; Heating;
DOI:10.1016/S0968-0896(01)00367-4

Reference yield:

: 100-39-0
benzyl bromide

: 321125-48-8
1-benzyloxy-2-methoxy-4-[2-nitroprop-1-enyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 16 h / 20 °C

2.1: ammonium acetate / toluene / 2 h / Dean-Stark; Reflux

2.2: 36 h / Reflux; Dean-Stark

With ammonium acetate; potassium carbonate; In acetone; toluene;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 321125-48-8
1-benzyloxy-2-methoxy-4-[2-nitroprop-1-enyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 16 h / 20 °C

2.1: ammonium acetate / toluene / 2 h / Dean-Stark; Reflux

2.2: 36 h / Reflux; Dean-Stark

With ammonium acetate; potassium carbonate; In acetone; toluene;