ALPHA-METHYL-(3-BENZYLOXY)BENZYL ALCOHOL

Base Information

• Chemical Name: ALPHA-METHYL-(3-BENZYLOXY)BENZYL ALCOHOL
• CAS No.: 320727-36-4
• Molecular Formula: C15H16 O2
• Molecular Weight: 228.291
• Hs Code.: 2909499000
• Mol file: 320727-36-4.mol

Synonyms:ALPHA-METHYL-(3-BENZYLOXY)BENZYL ALCOHOL

Chemical Property of ALPHA-METHYL-(3-BENZYLOXY)BENZYL ALCOHOL

Chemical Property:

• Vapor Pressure: 3.57E-06mmHg at 25°C
• Refractive Index: 1.582
• Boiling Point: 371.4°C at 760 mmHg
• PKA: 14.36±0.20(Predicted)
• Flash Point: 164.7°C
• PSA: 29.46000
• Density: 1.112g/cm³
• LogP: 3.31890

Purity/Quality:

98%,99%, ^*data from raw suppliers

ALPHA-METHYL-(3-BENZYLOXY)BENZYLALCOHOL ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ALPHA-METHYL-(3-BENZYLOXY)BENZYL ALCOHOL

There total 5 articles about ALPHA-METHYL-(3-BENZYLOXY)BENZYL ALCOHOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-[3-(phenylmethoxy)phenyl]ethan-1-one (34068-01-4) → 1-(3'-benzyloxyphenyl)ethanol (320727-36-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 1h;

DOI:10.1071/CH03027

Reference yield:

benzyl bromide (100-39-0) → 1-(3'-benzyloxyphenyl)ethanol (320727-36-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / potassium carbonate / dimethylformamide / 12 h / Heating

2: 99 percent / lithium aluminium hydride / diethyl ether / 1 h

With lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; N,N-dimethyl-formamide;

DOI:10.1071/CH03027

Reference yield:

3-Bromophenol (591-20-8) → 1-(3'-benzyloxyphenyl)ethanol (320727-36-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: K₂CO₃ / acetone / Heating

2.1: n-BuLi / -78 °C

2.2: 60 °C

With n-butyllithium; potassium carbonate; In acetone;

DOI:10.1016/j.bmcl.2004.04.058

upstream raw materials:

3-(benzyloxy)phenyl bromide

acetaldehyde

1-[3-(phenylmethoxy)phenyl]ethan-1-one

3-Hydroxyacetophenone

Downstream raw materials:

ethyl (2S)-2-(3'-benzyloxy-α'-methylbenzyloxy)propanoate

(α'R,2S)-2-(3'-benzyloxy-α'-methylbenzyloxy)propan-1-ol

(α'S,2S)-2-(3'-benzyloxy-α'-methylbenzyloxy)propan-1-ol

(α'R,2S)-2-(3'-benzyloxy-α'-methylbenzyloxy)propanal

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