Technology Process of C39H44O10
There total 5 articles about C39H44O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide; potassium hydride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
at 25 ℃;
for 4h;
DOI:10.1021/ja00107a009
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu4NBH4
2: 76 percent / KH, n-Bu4NI / diethyl ether; hexamethylphosphoric acid triamide / 4 h / 25 °C
With
dmap; tetra-(n-butyl)ammonium iodide; potassium hydride; tetrabutylammonium borohydride; Dess-Martin periodane;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1021/ja00107a009
- Guidance literature:
-
Multi-step reaction with 3 steps
1: p-toluenesulfonic acid / methanol / 48 h / 25 °C
2: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu4NBH4
3: 76 percent / KH, n-Bu4NI / diethyl ether; hexamethylphosphoric acid triamide / 4 h / 25 °C
With
dmap; tetra-(n-butyl)ammonium iodide; potassium hydride; tetrabutylammonium borohydride; Dess-Martin periodane; toluene-4-sulfonic acid;
In
methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1021/ja00107a009