(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Base Information

Chemical Name:(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid
CAS No.:1198281-48-9
Molecular Formula:C₂₅H₂₄BrNO₄
Molecular Weight:482.374
Hs Code.:

Synonyms:(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

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Chemical Property of (3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Chemical Property:

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Technology Process of (3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

There total 5 articles about (3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1198281-50-3
(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride

: 1198281-48-9
(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Guidance literature:: (3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride; With methanol; lithium hydroxide; In tetrahydrofuran;

In tetrahydrofuran; methanol; pH=7; Acidic conditions;

Reference yield:

: 1182351-81-0
[3-(4-bromo-2-formyl-phenoxy)-phenyl]-acetic acid

: 1198281-48-9
(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium cyanoborohydride; acetic acid / dichloromethane / 0.17 h / 20 °C

2.1: triethylamine / dichloromethane

3.1: methanol; lithium hydroxide / tetrahydrofuran

3.2: pH 7 / Acidic conditions

With methanol; sodium cyanoborohydride; acetic acid; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 621-37-4
m-hydroxyphenylacetic acid

: 1198281-48-9
(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 - 70 °C

2.1: sodium cyanoborohydride; acetic acid / dichloromethane / 0.17 h / 20 °C

3.1: triethylamine / dichloromethane

4.1: methanol; lithium hydroxide / tetrahydrofuran

4.2: pH 7 / Acidic conditions

With methanol; sodium hydride; sodium cyanoborohydride; acetic acid; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;