(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride

Base Information

Chemical Name:(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride
CAS No.:1198281-50-3
Molecular Formula:C₂₇H₂₆BrNO₅
Molecular Weight:524.411
Hs Code.:

Synonyms:(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride

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Chemical Property of (3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride

Chemical Property:

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Technology Process of (3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride

There total 4 articles about (3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1198281-49-0
{3-[4-bromo-2-(phenethylamino-methyl)-phenoxy]-phenyl}-acetic acid

: 75-36-5
acetyl chloride

: 1198281-50-3
(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 93777-26-5
5-bromo-2-fluorobenzaldehyde

: 1198281-50-3
(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 - 70 °C

2: sodium cyanoborohydride; acetic acid / dichloromethane / 0.17 h / 20 °C

3: triethylamine / dichloromethane

With sodium hydride; sodium cyanoborohydride; acetic acid; triethylamine; In dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1182351-81-0
[3-(4-bromo-2-formyl-phenoxy)-phenyl]-acetic acid

: 1198281-50-3
(3-{2-[(acetyl-phenethyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid acetyl anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride; acetic acid / dichloromethane / 0.17 h / 20 °C

2: triethylamine / dichloromethane

With sodium cyanoborohydride; acetic acid; triethylamine; In dichloromethane;