2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt

Base Information

Chemical Name:2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt
CAS No.:1258855-43-4
Molecular Formula:C₂HF₃O₂*C₂₂H₂₂N₄O₂
Molecular Weight:488.466
Hs Code.:

Synonyms:2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt

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Chemical Property of 2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt

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Technology Process of 2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt

There total 7 articles about 2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1167416-06-9
1,1-dimethylethyl 6-(5-{3-cyano-4-[(1-methylethyl)oxy] phenyl}-1,2,4-oxadiazol-3-yl)-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate

: 76-05-1
trifluoroacetic acid

: 1258855-43-4
2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt

Guidance literature:: In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 258273-31-3
3-cyano-4-isopropoxybenzoic acid

: 1258855-43-4
2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / 4 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 3.5 h / 20 - 120 °C / Inert atmosphere

3: dichloromethane / 0 - 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1072948-37-8
3-cyano-4-[(1-methylethyl)oxy]benzoyl chloride

: 1258855-43-4
2-[(1-methylethyl)oxy]-5-[3-(2,3,4,5-tetrahydro-1H-3-benzazepin-6-yl)-1,2,4-oxadiazol-5-yl]benzonitrile mono-trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 3.5 h / 20 - 120 °C / Inert atmosphere

2: dichloromethane / 0 - 20 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;