1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol

Base Information

Chemical Name:1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol
CAS No.:496808-81-2
Molecular Formula:C₃₅H₄₆O₁₀Si
Molecular Weight:654.83
Hs Code.:

Synonyms:1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol

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Chemical Property of 1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol

Chemical Property:

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Technology Process of 1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol

There total 4 articles about 1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 98-88-4
benzoyl chloride

: 107-30-2
chloromethyl methyl ether

: 142534-54-1
1D-1-O-(tert-butyldiphenylsilyl)-myo-inositol

: 165689-86-1
1D-1-O-(tert-butyldiphenylsilyl)-2,5,6-O-tris(methoxymethylene)-myo-inositol

: 496808-81-2
1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol

Guidance literature:: benzoyl chloride; 1D-1-O-(tert-butyldiphenylsilyl)-myo-inositol; With pyridine;

chloromethyl methyl ether; With N-ethyl-N,N-diisopropylamine;

With methylamine;
DOI:10.1021/jo0206418

Reference yield:

: 331679-26-6
2,3-O-(D-1,7,7-trimethylbicyclo[2.2.1]hept-6-ylidene)-D-myo-inositol

: 496808-81-2
1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / imidazole

2.1: 90 percent / HSCH₂CH₂OH; BF₃*Et₂O

3.1: pyridine / CH₂Cl₂ / 1 h / -50 °C

3.2: diisopropylethylamine

3.3: 31 percent / methylamine / methanol / 48 h / 20 °C

With pyridine; 1H-imidazole; boron trifluoride diethyl etherate; 2-hydroxyethanethiol; In dichloromethane;
DOI:10.1021/jo0206418

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 496808-81-2
1D-5-O-benzoyl-1-(tert-butyldiphenylsilyl)-2,4,6-O-tris(methoxymethylene)-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / imidazole

2.1: 90 percent / HSCH₂CH₂OH; BF₃*Et₂O

3.1: pyridine / CH₂Cl₂ / 1 h / -50 °C

3.2: diisopropylethylamine

3.3: 31 percent / methylamine / methanol / 48 h / 20 °C

With pyridine; 1H-imidazole; boron trifluoride diethyl etherate; 2-hydroxyethanethiol; In dichloromethane;
DOI:10.1021/jo0206418