C₂₉H₁₉F₂N₅O

Base Information

Chemical Name:C₂₉H₁₉F₂N₅O
CAS No.:1600566-54-8
Molecular Formula:C₂₉H₁₉F₂N₅O
Molecular Weight:491.5
Hs Code.:

C<sub>29</sub>H<sub>19</sub>F<sub>2</sub>N<sub>5</sub>O

Synonyms:C₂₉H₁₉F₂N₅O

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Chemical Property of C₂₉H₁₉F₂N₅O

Chemical Property:

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Technology Process of C₂₉H₁₉F₂N₅O

There total 9 articles about C₂₉H₁₉F₂N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1600566-51-5
3-(3-fluorophenyl)-6-((4-fluorophenyl)(hydroxy)(1-methyl-1H-imidazol-5-yl)methyl)-8-methylquinoline-2,4-dicarbonitrile

: 1600566-54-8
C₂₉H₁₉F₂N₅O

: 1600566-53-7
C₂₉H₁₉F₂N₅O

Guidance literature:: With chiral HPLC (Chiralcel OD, 80percent heptane/20percent EtOH); In ethanol; n-heptane; Resolution of racemate;

Reference yield:

: 1121-86-4
1-Fluoro-3-iodobenzene

: 1600566-54-8
C₂₉H₁₉F₂N₅O

: 1600566-53-7
C₂₉H₁₉F₂N₅O

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate; copper(l) iodide / 1,4-dioxane / 20 °C / Inert atmosphere

2.1: sodium hydroxide / water / 0.17 h / 65 °C

3.1: trichlorophosphate / 1 h / 70 °C

3.2: 3 h / 105 °C

4.1: tetrahydrofuran / 0.03 h / Inert atmosphere; Cooling with acetone-dry ice

4.2: 1.17 h / -78 °C / Inert atmosphere

4.3: Inert atmosphere

5.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc; XPhos / N,N-dimethyl acetamide / 1.5 h / 120 °C / Inert atmosphere

6.1: chiral HPLC (Chiralcel OD, 80percent heptane/20percent EtOH) / ethanol; n-heptane / Resolution of racemate

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; caesium carbonate; sodium hydroxide; zinc; XPhos; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol; n-heptane; N,N-dimethyl acetamide; water;

Reference yield:

: 1600563-24-3
6-bromo-2,4-dichloro-3-(3-fluorophenyl)-8-methylquinoline

: 1600566-54-8
C₂₉H₁₉F₂N₅O

: 1600566-53-7
C₂₉H₁₉F₂N₅O

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0.03 h / Inert atmosphere; Cooling with acetone-dry ice

1.2: 1.17 h / -78 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc; XPhos / N,N-dimethyl acetamide / 1.5 h / 120 °C / Inert atmosphere

3.1: chiral HPLC (Chiralcel OD, 80percent heptane/20percent EtOH) / ethanol; n-heptane / Resolution of racemate

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc; XPhos; In tetrahydrofuran; ethanol; n-heptane; N,N-dimethyl acetamide;