2-ethyl-3-nitrobenzeneamine

Base Information

Chemical Name:2-ethyl-3-nitrobenzeneamine
CAS No.:90007-09-3
Molecular Formula:C₈H₁₀N₂O₂
Molecular Weight:166.18
Hs Code.:

Synonyms:2-ethyl-3-nitrobenzeneamine

Suppliers and Price of 2-ethyl-3-nitrobenzeneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-ethyl-3-nitrobenzeneamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-ethyl-3-nitrobenzeneamine

There total 3 articles about 2-ethyl-3-nitrobenzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 13985-56-3
2-ethyl-1,3-dinitrobenzene

: 90007-09-3
2-ethyl-3-nitrobenzeneamine

Guidance literature:: With formic acid; triethylamine; palladium on activated charcoal; In acetonitrile; for 0.416667h; Heating;
DOI:10.1002/hlca.200490060

Reference yield:

: 13985-60-9
2-ethyl-1,3,5-trinitrobenzene

: 90007-09-3
2-ethyl-3-nitrobenzeneamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 48 percent / ammonia; H₂S / dioxane / 35 - 40 °C

2.1: NaNO₂; AcOH; H₂SO₄ / H₂O / 1 h / 20 - 25 °C

2.2: 76 percent / Cu₂O / ethanol; H₂O / 1.5 h / 20 °C

3.1: 81 percent / formic acid; Et₃N / Pd/C / acetonitrile / 0.42 h / Heating

With formic acid; sulfuric acid; hydrogen sulfide; ammonia; acetic acid; triethylamine; sodium nitrite; palladium on activated charcoal; In 1,4-dioxane; water; acetonitrile;
DOI:10.1002/hlca.200490060

Reference yield:

: 702642-25-9
4-ethyl-3,5-dinitrobenzeneamine

: 90007-09-3
2-ethyl-3-nitrobenzeneamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaNO₂; AcOH; H₂SO₄ / H₂O / 1 h / 20 - 25 °C

1.2: 76 percent / Cu₂O / ethanol; H₂O / 1.5 h / 20 °C

2.1: 81 percent / formic acid; Et₃N / Pd/C / acetonitrile / 0.42 h / Heating

With formic acid; sulfuric acid; acetic acid; triethylamine; sodium nitrite; palladium on activated charcoal; In water; acetonitrile;
DOI:10.1002/hlca.200490060