Technology Process of 2,5-bis-(phenylhydroxymethyl)-3,4-bis-(dodecyloxy)thiophene
There total 5 articles about 2,5-bis-(phenylhydroxymethyl)-3,4-bis-(dodecyloxy)thiophene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N,N,N,N,-tetramethylethylenediamine;
In
tetrahydrofuran; hexane;
for 1h;
Heating;
DOI:10.1016/j.tet.2004.09.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 67 percent / p-toluenesulfonic acid / toluene / 90 °C
2: 33 percent / N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran / 1 h / Heating
With
N,N,N,N,-tetramethylethylenediamine; toluene-4-sulfonic acid;
In
tetrahydrofuran; hexane; toluene;
DOI:10.1016/j.tet.2004.09.008
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 56 percent / copper chromite; quinoline / 4 h / 160 °C
2: 67 percent / p-toluenesulfonic acid / toluene / 90 °C
3: 33 percent / N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran / 1 h / Heating
With
quinoline; copper chromite; N,N,N,N,-tetramethylethylenediamine; toluene-4-sulfonic acid;
In
tetrahydrofuran; hexane; toluene;
DOI:10.1016/j.tet.2004.09.008