(E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate

Base Information

Chemical Name:(E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate
CAS No.:1310809-29-0
Molecular Formula:C₁₇H₂₂N₂O₆
Molecular Weight:350.371
Hs Code.:

Synonyms:(E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate

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Chemical Property of (E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate

Chemical Property:

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Technology Process of (E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate

There total 5 articles about (E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1310809-24-5
C₉H₁₆N₂O₄

: 501-53-1,94274-21-2
benzyl chloroformate

: 1310809-29-0
(E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1021/ja201597b

Reference yield:

: C₁₄H₂₄N₂O₆

: 1310809-29-0
(E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

2: triethylamine / dichloromethane / 5 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ja201597b

Reference yield:

: 1310809-22-3
(E)-methyl 4-(benzoyloxy(4-(tert-butoxycarbonylamino)butyl)amino)-4-oxobut-2-enoate

: 1310809-29-0
(E)-methyl 4-((4-(benzyloxycarbonylamino)butyl)(hydroxy)amino)-4-oxobut-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol / 0.5 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

3: triethylamine / dichloromethane / 5 h / 0 °C

With potassium carbonate; triethylamine; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/ja201597b