2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-one

Base Information

• Chemical Name: 2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-one
• CAS No.: 915708-12-2
• Molecular Formula: C₂₇H₃₈O₆
• Molecular Weight: 458.595

Synonyms:2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-one

Chemical Property of 2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-one

Chemical Property:

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Technology Process of 2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-one

There total 1 articles about 2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-diazo-6-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-9-(4-methoxy-benzyloxymethyl)-dec-9-ene-2,5-dione (915708-11-1) → 2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.01,5]undecan-8-one + 2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.01,5]undecan-8-one (915708-12-2)

Guidance literature:

With Rh₂[(S)-BPTV]4; In various solvent(s); at -40 ℃; for 3h;

DOI:10.1002/anie.200602056

Reference yield:

2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.01,5]undecan-8-one (915708-12-2) → 3-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8a-(4-methoxy-benzyloxymethyl)-6-methyl-2,3,4,5,8,8a-hexahydro-1H-azulen-3a-ol (915708-15-5)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / 1 h / -20 °C

2: SOCl₂; DMPU / 0 - 20 °C

3: Na / diethyl ether / 12 h / Heating

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; thionyl chloride; sodium; In tetrahydrofuran; diethyl ether;

DOI:10.1002/anie.200602056

Reference yield:

2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-11-oxa-tricyclo[5.3.1.01,5]undecan-8-one (915708-12-2) → 8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.01,5]undecane (915708-14-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / -20 °C

2: SOCl₂; DMPU / 0 - 20 °C

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; thionyl chloride; In tetrahydrofuran;

DOI:10.1002/anie.200602056

upstream raw materials:

1-diazo-6-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-9-(4-methoxy-benzyloxymethyl)-dec-9-ene-2,5-dione

Downstream raw materials:

2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecan-8-ol

3-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-8a-(4-methoxy-benzyloxymethyl)-6-methyl-2,3,4,5,8,8a-hexahydro-1H-azulen-3a-ol

8-chloro-2-(2,2-diethyl-4-methyl-[1,3]dioxolan-4-yl)-5-(4-methoxy-benzyloxymethyl)-8-methyl-11-oxa-tricyclo[5.3.1.0^1,5]undecane

deacetylpseudolaric acid A

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