Benzoicacid, 2,4-dichloro-, 2-benzoyl-1-(1,1-dimethylethyl)hydrazide

Base Information

• Chemical Name: Benzoicacid, 2,4-dichloro-, 2-benzoyl-1-(1,1-dimethylethyl)hydrazide
• CAS No.: 112226-97-8
• Molecular Formula: C₁₈H₁₈Cl₂N₂O₂
• Molecular Weight: 365.259
• Mol file: 112226-97-8.mol

Synonyms:

Chemical Property of Benzoicacid, 2,4-dichloro-, 2-benzoyl-1-(1,1-dimethylethyl)hydrazide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.275g/cm³

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoicacid, 2,4-dichloro-, 2-benzoyl-1-(1,1-dimethylethyl)hydrazide

There total 4 articles about Benzoicacid, 2,4-dichloro-, 2-benzoyl-1-(1,1-dimethylethyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzoyl-2-tert-butylhydrazine (17473-79-9) + 2,4-dichlorobenzoyl chloride (89-75-8) → N'-t-butyl-N-benzoyl-N'-(2,4-dichlorobenzoyl)hydrazine (112226-97-8)

Guidance literature:

With sodium hydroxide; In diethyl ether; at 20 ℃; for 3h;

DOI:10.1002/ps.2780410210

Reference yield:

2,4 dichlorobenzoic acid (50-84-0) → N'-t-butyl-N-benzoyl-N'-(2,4-dichlorobenzoyl)hydrazine (112226-97-8)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / 12 h / Heating

2: aq. NaOH / diethyl ether / 3 h / 20 °C

With sodium hydroxide; thionyl chloride; In diethyl ether; 1: Chlorination / 2: Substitution;

DOI:10.1002/ps.2780410210

Reference yield:

benzoyl chloride (98-88-4) → N'-t-butyl-N-benzoyl-N'-(2,4-dichlorobenzoyl)hydrazine (112226-97-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 84.4 percent / aq. NaOH / diethyl ether / 1 h / 20 °C

2: aq. NaOH / diethyl ether / 3 h / 20 °C

With sodium hydroxide; In diethyl ether; 1: Substitution / 2: Substitution;

DOI:10.1002/ps.2780410210

upstream raw materials:

1-benzoyl-2-tert-butylhydrazine

2,4-dichlorobenzoyl chloride

2,4 dichlorobenzoic acid

benzoyl chloride

Refernces

• 1、 -. "Insecticidal N'-substituted-N,N'-diacylhydrazines". . . Retrieved 2008/06/13.