phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside
CAS No.:612844-09-4
Molecular Formula:C₂₅H₂₃Cl₆NO₈S
Molecular Weight:710.244
Hs Code.:

Synonyms:phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside

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Chemical Property of phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside

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Technology Process of phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside

There total 1 articles about phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: phenyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-galactopyranoside

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 612844-09-4
phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside

Guidance literature:: With pyridine; for 0.0833333h;
DOI:10.1021/jo8027888

Reference yield: 93.0%

: n-hexyl-2,3,4-tri-O-acetyl-β-D-glucopyranoside

: 612844-09-4
phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside

: Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-hexyloxy-2-[(2S,4aR,6R,7R,8R,8aR)-2-phenyl-7-(2,2,2-trichloro-ethoxycarbonylamino)-8-(2,2,2-trichloro-ethoxycarbonyloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxymethyl]-tetrahydro-pyran-3-yl ester

: Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-hexyloxy-2-[(2S,4aR,6S,7R,8R,8aR)-2-phenyl-7-(2,2,2-trichloro-ethoxycarbonylamino)-8-(2,2,2-trichloro-ethoxycarbonyloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxymethyl]-tetrahydro-pyran-3-yl ester

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/S0040-4039(03)01647-2

Reference yield: 85.0%

: C₈₈H₉₂O₁₇

: 612844-09-4
phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside

: p-methoxyphenyl [4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranosyl]-(1→3)-(2,4,6-tri-O-benzyl-α-D-galactopyranosyl)-(1 → 4)-(2,3,6-tri-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: C₈₈H₉₂O₁₇; phenyl 4,6-O-benzylidene-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbamoyl)-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-galactopyranoside; With N-iodo-succinimide; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;

With trifluorormethanesulfonic acid; In dichloromethane; at -80 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.orglett.9b01372