5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine

Base Information

Chemical Name:5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine
CAS No.:204515-54-8
Molecular Formula:C₃₂H₃₂N₄O₆
Molecular Weight:568.629
Hs Code.:

Synonyms:5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine

Suppliers and Price of 5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine

There total 4 articles about 5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 204515-53-7
8-Oxo-2'-deoxy-7,8-dihydrocarbainosine

: 204515-54-8
5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine

Guidance literature:: With pyridine;
DOI:10.1021/tx9701539

Reference yield:

: 57345-51-4
(1S,2R,4R)-4-(6-amino-9H-purin-9-yl)-2-(hydroxymethyl)cyclopentan-1-ol

: 204515-54-8
5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine

Guidance literature:: Multi-step reaction with 5 steps

1: Br₂ / acetate buffer / pH 4

2: 61 percent / Na / dimethylformamide / 10 h / 80 °C

3: 100 percent / H₂ / Pd/C / methanol / 3 h / 50 °C / 2585.74 Torr

4: 86 percent / adenosine deaminase / H₂O / 192 h

5: 67 percent / pyridine

With pyridine; hydrogen; bromine; sodium; adenosine deaminase; palladium on activated charcoal; In methanol; acetate buffer; water; N,N-dimethyl-formamide; 1: Bromination / 2: Etherification / 3: Reductive debenzylation / 4: Enzymatic deamination / 5: Substitution;
DOI:10.1021/tx9701539

Reference yield:

: 204515-50-4
8-Bromo-2'-deoxyaristeromycin

: 204515-54-8
5'-O-DMT-8-oxo-7,8-dihydro-2'-deoxycarbainosine

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / Na / dimethylformamide / 10 h / 80 °C

2: 100 percent / H₂ / Pd/C / methanol / 3 h / 50 °C / 2585.74 Torr

3: 86 percent / adenosine deaminase / H₂O / 192 h

4: 67 percent / pyridine

With pyridine; hydrogen; sodium; adenosine deaminase; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide; 1: Etherification / 2: Reductive debenzylation / 3: Enzymatic deamination / 4: Substitution;
DOI:10.1021/tx9701539