N-{2-[5,8-di(tert-butyl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl]ethyl}-N'-(2,2-diphenylethyl)-succinamide

Base Information

Chemical Name:N-{2-[5,8-di(tert-butyl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl]ethyl}-N'-(2,2-diphenylethyl)-succinamide
CAS No.:575450-10-1
Molecular Formula:C₄₀H₄₅N₃O₄
Molecular Weight:631.815
Hs Code.:

Synonyms:N-{2-[5,8-di(tert-butyl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl]ethyl}-N'-(2,2-diphenylethyl)-succinamide

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Chemical Property of N-{2-[5,8-di(tert-butyl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl]ethyl}-N'-(2,2-diphenylethyl)-succinamide

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Technology Process of N-{2-[5,8-di(tert-butyl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl]ethyl}-N'-(2,2-diphenylethyl)-succinamide

There total 2 articles about N-{2-[5,8-di(tert-butyl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl]ethyl}-N'-(2,2-diphenylethyl)-succinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 137379-56-7
4-((2,2-diphenylethyl)amino)-4-oxobutanoic acid

: 2-(2-aminoethyl)-5,8-di-tert-butylbenzo[de]isoquinoline-1,3-dione

: 575450-10-1
N-{2-[5,8-di(tert-butyl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl]ethyl}-N'-(2,2-diphenylethyl)-succinamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1021/ja0352552

Reference yield:

: 3963-62-0
2,2-Diphenylethylamine

: 575450-10-1
N-{2-[5,8-di(tert-butyl)-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl]ethyl}-N'-(2,2-diphenylethyl)-succinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / 16 h

2: 93 percent / 4-(dimethylamino)pyridine; 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl / CH₂Cl₂ / 20 °C

With pyridine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/ja0352552