1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate

Base Information

Chemical Name:1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate
CAS No.:1608105-38-9
Molecular Formula:C₂₈H₂₆O₇
Molecular Weight:474.51
Hs Code.:

Synonyms:1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate

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Chemical Property of 1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate

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Technology Process of 1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate

There total 6 articles about 1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1608105-90-3
C₂₃H₂₀O₄

: 108-59-8
malonic acid dimethyl ester

: 1608105-38-9
1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate

Guidance literature:: With titanium tetrachloride; triethylamine; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/j.tetlet.2014.03.089

Reference yield:

: 36901-75-4
(2-bromobenzyl)triphenylphosphonium bromide

: 1608105-38-9
1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / tetrahydrofuran

2: n-butyllithium / tetrahydrofuran

3: water / 20 °C / Alkaline conditions

4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 °C

5: titanium tetrachloride; triethylamine / dichloromethane / 3 h / 0 °C

With dmap; n-butyllithium; titanium tetrachloride; sodium hydride; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; 1: |Wittig Olefination;
DOI:10.1016/j.tetlet.2014.03.089

Reference yield:

: 92434-54-3
1-bromo-2-(4-methoxystyryl)benzene

: 1608105-38-9
1,1-dimethyl 2-phenyl 2-(2-(4-methoxyphenylethyl)phenyl)ethene-1,1,2-tricarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: n-butyllithium / tetrahydrofuran

2: water / 20 °C / Alkaline conditions

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 °C

4: titanium tetrachloride; triethylamine / dichloromethane / 3 h / 0 °C

With dmap; n-butyllithium; titanium tetrachloride; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2014.03.089