4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene

Base Information

Chemical Name:4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene
CAS No.:1356472-16-6
Molecular Formula:C₃₃H₃₃NO₉
Molecular Weight:587.626
Hs Code.:

Synonyms:4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene

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Technology Process of 4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene

There total 2 articles about 4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1356472-53-1
2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

: 1356472-16-6
4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 5h; Reflux;
DOI:10.1039/c1nj20841a

Reference yield:

: 1356472-15-5
4-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene

: 1356472-16-6
4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide

2: 18-crown-6 ether; potassium carbonate / acetone / 5 h / Reflux

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide; acetone; 2: Williamson etherification;
DOI:10.1039/c1nj20841a

Reference yield:

: 1356472-16-6
4-(2-(2-(2-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-nitrobenzene

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 2896-67-5
2-methyl-6-methoxyphenol

Guidance literature:: With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide;
DOI:10.1039/c1nj20841a