3-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-4-enal-(ethyl-methyl-acetal)

Base Information

• Chemical Name: 3-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-4-enal-(ethyl-methyl-acetal)
• CAS No.: 102376-12-5
• Molecular Formula: C₂₀H₃₆O₃
• Molecular Weight: 324.504

Synonyms:3-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-4-enal-(ethyl-methyl-acetal)

Chemical Property of 3-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-4-enal-(ethyl-methyl-acetal)

Chemical Property:

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Technology Process of 3-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-4-enal-(ethyl-methyl-acetal)

There total 1 articles about 3-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-4-enal-(ethyl-methyl-acetal) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-crotonaldehyde dimethylacetal (101725-96-6) + ethyl vinyl ether (109-92-2,25104-37-4) → 3-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-4-enal-(ethyl-methyl-acetal) (102376-12-5)

Guidance literature:

With 1-ethyl-3-methylimidazolium hydrogensulfate; at 45 ℃;

DOI:10.1016/j.tet.2010.11.005

Reference yield:

3-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-4-enal-(ethyl-methyl-acetal) (102376-12-5) → E,E-6-(2',6',6'-trimethylcyclohex-1'-en-1'-yl)-4-methyl-hexa-2,4-dien-1-al (5560-91-8)

Guidance literature:

With sodium acetate; acetic acid; In water; at 95 ℃; stereoselective reaction;

DOI:10.1016/j.tet.2010.11.005

upstream raw materials:

methanol

2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-crotonaldehyde dimethylacetal

ethyl vinyl ether

Downstream raw materials:

E,E-6-(2',6',6'-trimethylcyclohex-1'-en-1'-yl)-4-methyl-hexa-2,4-dien-1-al

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