N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

Base Information

Chemical Name:N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine
CAS No.:386210-68-0
Molecular Formula:C₅₁H₇₃Cl₂NO₆
Molecular Weight:867.05
Hs Code.:

Synonyms:N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

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Chemical Property of N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

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Technology Process of N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

There total 1 articles about N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

: 3β-amino-5α-cholestane hydrochloride

: 252934-37-5
C₂₄H₂₄Cl₂O₇

: 386210-68-0
N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

Guidance literature:: With sodium tris(acetoxy)borohydride; triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 24h;
DOI:10.1016/S0968-0896(01)00152-3

Reference yield: 84.0%

: 207743-06-4
3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid

: 386210-68-0
N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

: 386210-72-6
N-(5α-cholestan-3β-yl)-N-[6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenyl]-3,3-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-2-propenamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/S0968-0896(01)00152-3

Reference yield: 72.0%

: 386210-68-0
N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

: N-(5α-cholestan-3β-yl)-6,6-bis(3'-carboxy-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

Guidance literature:: N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine; With potassium cyanide; potassium carbonate; In tetrahydrofuran; methanol; water; at 75 ℃; for 4h;

With water; at 75 ℃; for 1h;
DOI:10.1016/S0968-0896(01)00152-3