3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid

Base Information

Chemical Name:3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid
CAS No.:207743-06-4
Molecular Formula:C₂₁H₁₈Cl₂O₈
Molecular Weight:469.275
Hs Code.:

Synonyms:3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid

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Chemical Property of 3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid

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Technology Process of 3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid

There total 1 articles about 3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2-(trimethylsilyl)ethyl 3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoate

: 207743-06-4
3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1.5h;
DOI:10.1021/jm9800595

Reference yield: 89.1%

: 2206-20-4
3α-amino-5α-cholestane

: 207743-06-4
3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid

: N-(5α-cholestan-3α-yl)-3,3-bis(3-chloro-4-methoxy-5-methoxycarbonylphenyl)-2-propenamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 51h;
DOI:10.1016/S0968-0896(99)00269-2

Reference yield: 84.0%

: 207743-06-4
3',3''-dichloro-4',4''-dimethoxy-5',5''-bis(methoxycarbonyl)-3,3-diphenylpropenoic acid

: 386210-68-0
N-(5α-cholestan-3β-yl)-6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenylamine

: 386210-72-6
N-(5α-cholestan-3β-yl)-N-[6,6-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-5-hexenyl]-3,3-bis(3'-methoxycarbonyl-5'-chloro-4'-methoxyphenyl)-2-propenamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/S0968-0896(01)00152-3