bis(tricyclohexylphosphine)indium trihydride

Base Information

Chemical Name:bis(tricyclohexylphosphine)indium trihydride
CAS No.:263332-03-2
Molecular Formula:C₃₆H₆₉InP₂
Molecular Weight:678.711
Hs Code.:

Synonyms:bis(tricyclohexylphosphine)indium trihydride

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Chemical Property of bis(tricyclohexylphosphine)indium trihydride

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Technology Process of bis(tricyclohexylphosphine)indium trihydride

There total 2 articles about bis(tricyclohexylphosphine)indium trihydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 220995-57-3
tricyclohexylphosphineindium trihydride

: 2622-14-2
tricyclohexylphosphine

: 263332-03-2
bis(tricyclohexylphosphine)indium trihydride

Guidance literature:: In 1,2-dimethoxyethane; under Ar or N2; soln. of ligand in DME slowly added to stirred soln. ofIn complex (molar ratio 1:1) in DME at -70°C; warmed to -30°C; stirred for 2 h; volatiles removed in vac.; solid washed with cold Et2O; extd. with cold(-20°C) DME; concd. in vac.; filtered; filtrate stood at -30°C;
DOI:10.1039/a908418e

Reference yield: 63.0%

: 153594-82-2
trimethylamineindium trihydrate

: 2622-14-2
tricyclohexylphosphine

: 263332-03-2
bis(tricyclohexylphosphine)indium trihydride

Guidance literature:: In diethyl ether; under Ar or N2; soln. of ligand in Et2O slowly added to soln. of In complex (molar ratio 2:1) in Et2O at -70°C; warmed to -30°C; stirred for 2 h; volatiles removed in vac.; solid washed with cold Et2O; extd. with cold(-20°C) DME; filtered; filtrate stood at -30°C;
DOI:10.1039/a908418e