α-butylbenzeneacetaldehyde

Base Information

• Chemical Name: α-butylbenzeneacetaldehyde
• CAS No.: 73083-29-1
• Molecular Formula: C₁₂H₁₆O
• Molecular Weight: 176.258
• Mol file: 73083-29-1.mol

Synonyms:α-butylbenzeneacetaldehyde

Chemical Property of α-butylbenzeneacetaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-butylbenzeneacetaldehyde

There total 8 articles about α-butylbenzeneacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

triphenylaluminium (841-76-9) + hexanal (66-25-1) → α-butylbenzeneacetaldehyde (73083-29-1)

Guidance literature:

With isoxazolidine; In dichloromethane; at 0 ℃; for 2h; Reagent/catalyst; Mechanism; Inert atmosphere;

DOI:10.1002/ejoc.201500308

Reference yield: 70.0%

pyridine (110-86-1) + chromium(VI) oxide + 2-benzene-2-butylethanol (25755-73-1) → α-butylbenzeneacetaldehyde (73083-29-1)

Guidance literature:

pyridine; chromium(VI) oxide; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;

2-benzene-2-butylethanol; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;

DOI:10.1021/ol900863d

Reference yield:

diphenylboronchloride (3677-81-4) + hex-1-yne (693-02-7) → caprophenone (942-92-7) + α-butylbenzeneacetaldehyde (73083-29-1)

Guidance literature:

With sodium hydroxide; sodium dihydrogenphosphate; dihydrogen peroxide; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) 130 deg C, 1.5 h, 2.) 0 deg C, 2 h, pentane;

upstream raw materials:

1-bromo-butane

phenylacetonitrile

diphenylboronchloride

hex-1-yne

Downstream raw materials:

(+/-)-4-phenyl-oct-2Ξ-ene

4-butyl-1,2-diphenylnaphthalene

(Z)-3-(2-phenylhex-1-en-1-yl)oxazolidin-2-one