2,2,4,4-Tetraphenyl-3-butenaldehyde

Base Information

• Chemical Name: 2,2,4,4-Tetraphenyl-3-butenaldehyde
• CAS No.: 41326-74-3
• Molecular Formula: C₂₈H₂₂O
• Molecular Weight: 374.482
• Mol file: 41326-74-3.mol

Synonyms:2,2,4,4-Tetraphenyl-3-butenaldehyde

Chemical Property of 2,2,4,4-Tetraphenyl-3-butenaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2,4,4-Tetraphenyl-3-butenaldehyde

There total 6 articles about 2,2,4,4-Tetraphenyl-3-butenaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2-methyl-5,5,7,7-tetraphenyl-3-azahepta-3,6-diene (111220-85-0) → 2,2,4,4-Tetraphenyl-3-butenaldehyde (41326-74-3) + 1,1,2,2-Tetraphenylcyclopropanecarboxaldehyde (79236-77-4)

Guidance literature:

With acetophenone; In benzene; for 1h; Irradiation;

Reference yield:

bis(2,2-diphenylvinyl) ether (93620-51-0) → 1,1-Diphenylethylene (530-48-3) + benzophenone (119-61-9) + 1,1,4,4-tetraphenyl-1,3-butadiene (1450-63-1) + 2,2,4,4-Tetraphenyl-3-butenaldehyde (41326-74-3)

Guidance literature:

In benzene; for 0.2h; Product distribution; Quantum yield; Mechanism; Irradiation; var. solvents and time; var. λ used for photolysis; in presence of radical scavenger 2,6-di-tert-butyl-4-methylphenol; in presence of methanol and acetic acid; under oxygen pressure; crossover photolysis together with bis(2,2-di-p-tolylvinyl) ether;

DOI:10.1021/jo00224a050

Reference yield:

2,2,4,4-Tetraphenylbutenol-3 (41326-73-2) → 2,2,4,4-Tetraphenyl-3-butenaldehyde (41326-74-3)

Guidance literature:

With acetic anhydride;

DOI:10.1021/ja00788a013

upstream raw materials:

bis(2,2-diphenylvinyl) ether

2-methyl-5,5,7,7-tetraphenyl-3-azahepta-3,6-diene

2,2,4,4-Tetraphenylbutenol-3

2,2,4,4-Tetraphenyl-3-butensaeure

Downstream raw materials:

1,2,2,3-Tetraphenylcyclopropan-1-carboxaldehyd

1,1-Dicyano-2,2-diphenyl-3-(2,2-diphenylvinyl)cyclopropane

2-(1,2,2,3-Tetraphenyl-cyclopropylmethylene)-malononitrile

1-acetoxy-3,3,5,5-tetraphenyl-1-azapenta-1,4-diene