1,2-Dichlorobenzene-5-ide;iodozinc(1+)

Base Information

Chemical Name:1,2-Dichlorobenzene-5-ide;iodozinc(1+)
CAS No.:312692-85-6
Molecular Formula:C₆H₃Cl₂IZn
Molecular Weight:338.29
Hs Code.:
DSSTox Substance ID:DTXSID70404374
Mol file:312692-85-6.mol

Synonyms:312692-85-6;1,2-dichlorobenzene-5-ide;iodozinc(1+);3,4-dichlorophenylzinc iodide;DTXSID70404374;3,4-DICHLOROPHENYLZINCIODIDE

Suppliers and Price of 1,2-Dichlorobenzene-5-ide;iodozinc(1+)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3,4-Dichlorophenylzinc iodide solution 0.5M in THF
50ml
$ 166.00

Rieke Metals
3,4-Dichlorophenylzinciodide
100mL
$ 482.00

American Custom Chemicals Corporation
3,4-DICHLOROPHENYLZINC IODIDE 95.00%
1L
$ 7969.50

American Custom Chemicals Corporation
3,4-DICHLOROPHENYLZINC IODIDE 95.00%
500ML
$ 5428.50

American Custom Chemicals Corporation
3,4-DICHLOROPHENYLZINC IODIDE 95.00%
100ML
$ 2818.20

Total 8 raw suppliers

Chemical Property of 1,2-Dichlorobenzene-5-ide;iodozinc(1+)

Chemical Property:

Vapor Pressure:1.21mmHg at 25°C
Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：0.00000
Density:g/cm³
LogP:3.67680
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:335.79479
Heavy Atom Count:10
Complexity:177

Purity/Quality:

99% ^*data from raw suppliers

3,4-Dichlorophenylzinc iodide solution 0.5M in THF ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F,T,Xn
Statements: 11-19-23/24/25-36/37/38-40-36/37
Safety Statements: 16-26-28-33-36/37-45

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:C1=CC(=C(C=[C-]1)Cl)Cl.[Zn+]I

Technology Process of 1,2-Dichlorobenzene-5-ide;iodozinc(1+)

There total 1 articles about 1,2-Dichlorobenzene-5-ide;iodozinc(1+) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20555-91-3
3,4-dichloroiodobenzene

: 7440-66-6
zinc

: 312692-85-6
(3,4-dichlorophenyl)zinc(II) iodide

Guidance literature:: zinc; With lithium chloride; at 150 - 170 ℃; for 2h; Inert atmosphere; Schlenk technique;

With chloro-trimethyl-silane; ethylene dibromide; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Glovebox;

3,4-dichloroiodobenzene; In tetrahydrofuran; for 24h; Inert atmosphere; Glovebox; Reflux;
DOI:10.1021/jacs.8b03163

Reference yield: 74.0%

: 312692-85-6
(3,4-dichlorophenyl)zinc(II) iodide

: 65805-36-9
3-(2-iodoethoxy)prop-1-ene

: 3-(3,4-dichlorobenzyl)tetrahydrofuran

Guidance literature:: With 2,2':6,2''-terpyridine; nickel dibromide; In tetrahydrofuran; at 50 ℃; for 6h; Glovebox; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.8b00184

Reference yield:

: 312692-85-6
(3,4-dichlorophenyl)zinc(II) iodide

: 852546-91-9
N-phenyl-1-(2-vinylphenyl)methanimine

: 51229-51-7
4-acetylbenzyl bromide

: C₃₀H₂₅Cl₂NO

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; In tetrahydrofuran; toluene; at 20 ℃; for 12h; regioselective reaction; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1002/anie.202110459