1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone

Base Information

Chemical Name:1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone
CAS No.:189343-62-2
Molecular Formula:C₂₈H₂₅N₅O₂S₂
Molecular Weight:527.671
Hs Code.:

Synonyms:1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone

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Chemical Property of 1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone

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Technology Process of 1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone

There total 3 articles about 1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 2-Benzotriazol-1-yl-2-phenylsulfanyl-1-p-tolyl-ethanone

: 189343-62-2
1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone

Guidance literature:: With amberlyst-15; In benzene; for 12h; Heating;
DOI:10.1021/jo962291t

Reference yield:

: 99-75-2
4-methyl-benzoic acid methyl ester

: 189343-62-2
1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / n-BuLi / tetrahydrofuran; hexane / 12 h / -78 - 20 °C

2: 95 percent / Amberlyst-15 / benzene / 12 h / Heating

With n-butyllithium; amberlyst-15; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/jo962291t

Reference yield:

: 111198-03-9
1-((phenylthio)methyl)-1H-benzo[d][1,2,3]triazole

: 189343-62-2
1-(benzotriazol-1-yl)-1-(phenylthio)-p-methylacetophenone p-tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / n-BuLi / tetrahydrofuran; hexane / 12 h / -78 - 20 °C

2: 95 percent / Amberlyst-15 / benzene / 12 h / Heating

With n-butyllithium; amberlyst-15; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/jo962291t