methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate

Base Information

Chemical Name:methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate
CAS No.:1571083-20-9
Molecular Formula:C₂₅H₂₅N₃O₂
Molecular Weight:399.492
Hs Code.:

Synonyms:methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate

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Technology Process of methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate

There total 4 articles about methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1571083-18-5
methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-oxobutanoate

: 100-63-0
phenylhydrazine

: 1571083-20-9
methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate

Guidance literature:: In ethanol; for 3h; Reflux;
DOI:10.1016/j.tet.2014.01.070

Reference yield:

: 41532-84-7
2,3,3-trimethylbenzo[e]indole

: 1571083-20-9
methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: o-xylene / 1 h / 200 °C / Microwave irradiation

2: acetyl chloride / 1.5 h / Inert atmosphere; Reflux

3: dimethyl sulfoxide / 8 h / 50 °C

4: ethanol / 3 h / Reflux

With dimethyl sulfoxide; acetyl chloride; In ethanol; o-xylene;
DOI:10.1016/j.tet.2014.01.070

Reference yield:

: 1571083-09-4
12,12-dimethyl-10,12-dihydrobenzo[e]pyrido[1,2-a]indol-8(9H)-one

: 1571083-20-9
methyl 4-(1,1-dimethyl-1H-benzo[e]indol-2-yl)-4-(2-phenylhydrazinylidene)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride / 1.5 h / Inert atmosphere; Reflux

2: dimethyl sulfoxide / 8 h / 50 °C

3: ethanol / 3 h / Reflux

With dimethyl sulfoxide; acetyl chloride; In ethanol;
DOI:10.1016/j.tet.2014.01.070