(E)-cinnamyl o-nitrophenyl selenide

Base Information

• Chemical Name: (E)-cinnamyl o-nitrophenyl selenide
• CAS No.: 168326-76-9
• Molecular Formula: C₁₅H₁₃NO₂Se
• Molecular Weight: 318.234
• Mol file: 168326-76-9.mol

Synonyms:(E)-cinnamyl o-nitrophenyl selenide

Chemical Property of (E)-cinnamyl o-nitrophenyl selenide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-cinnamyl o-nitrophenyl selenide

There total 1 articles about (E)-cinnamyl o-nitrophenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

ortho-nitrophenyl selenocyanate (51694-22-5) + (2E)-3-phenyl-2-propen-1-ol (4407-36-7) → (E)-cinnamyl o-nitrophenyl selenide (168326-76-9)

Guidance literature:

With tributylphosphine; In tetrahydrofuran;

DOI:10.1039/b316502g

Reference yield: 65.0%

(E)-cinnamyl o-nitrophenyl selenide (168326-76-9) → 1-Phenyl-2-propen-1-ol (4393-06-0)

Guidance literature:

(E)-cinnamyl o-nitrophenyl selenide; With Cumene hydroperoxide; 4 A molecular sieve; vanadyl acetylacetonate; In dichloromethane; at -10 ℃; for 0.5h;

With tributylphosphine; In dichloromethane; at -10 ℃; for 0.0833333h;

DOI:10.1039/b316502g

Reference yield: 55.0%

diazoacetic acid ethyl ester (623-73-4) + (E)-cinnamyl o-nitrophenyl selenide (168326-76-9) → 2-(2-Nitro-phenylselanyl)-3-phenyl-pent-4-enoic acid ethyl ester

Guidance literature:

copper(I) triflate; (S,S)-2,2'-methylenebis(4-tert-butyl-2-oxazoline); In chloroform; at 0 ℃; for 24h;

DOI:10.1039/c39950001245

upstream raw materials:

ortho-nitrophenyl selenocyanate

(2E)-3-phenyl-2-propen-1-ol

Downstream raw materials:

(R)-1-phenylprop-2-en-1-ol

(1S)-1-phenylprop-2-en-1-ol

1-Phenyl-2-propen-1-ol