tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate

Base Information

Chemical Name:tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate
CAS No.:1620090-36-9
Molecular Formula:C₂₂H₂₅IN₂O₄S
Molecular Weight:540.422
Hs Code.:

Synonyms:tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate

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Technology Process of tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate

There total 3 articles about tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620090-31-4
tert-butyl-2-(4-(4-methylphenylsulfonamido)but-1-ynyl)phenylcarbamate

: 1620090-36-9
tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate

Guidance literature:: With iodine; potassium carbonate; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c4cc02466d

Reference yield:

: 161117-84-6
tert-butyl 2-iodophenylcarbamate

: 1620090-36-9
tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / triethylamine / 6 h / 20 °C

2: potassium carbonate; iodine / acetonitrile / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; iodine; potassium carbonate; In triethylamine; acetonitrile;
DOI:10.1039/c4cc02466d

Reference yield:

: 161040-05-7
N-(but-3-yn-1-yl)-4-methylbenzenesulfonamide

: 1620090-36-9
tert-butyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / triethylamine / 6 h / 20 °C

2: potassium carbonate; iodine / acetonitrile / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; iodine; potassium carbonate; In triethylamine; acetonitrile;
DOI:10.1039/c4cc02466d