methyl 3-methylene [(2,4-dimethyl-phenyl)-phosphinate ethyl ester]thiophene-2-carboxylate

Base Information

Chemical Name:methyl 3-methylene [(2,4-dimethyl-phenyl)-phosphinate ethyl ester]thiophene-2-carboxylate
CAS No.:1243142-03-1
Molecular Formula:C₁₇H₂₁O₄PS
Molecular Weight:352.391
Hs Code.:

Synonyms:methyl 3-methylene [(2,4-dimethyl-phenyl)-phosphinate ethyl ester]thiophene-2-carboxylate

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Chemical Property of methyl 3-methylene [(2,4-dimethyl-phenyl)-phosphinate ethyl ester]thiophene-2-carboxylate

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Technology Process of methyl 3-methylene [(2,4-dimethyl-phenyl)-phosphinate ethyl ester]thiophene-2-carboxylate

There total 1 articles about methyl 3-methylene [(2,4-dimethyl-phenyl)-phosphinate ethyl ester]thiophene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 589-57-1
diethyl phosphorylchloridite

: 34589-46-3
(2,4-dimethylphenyl)magnesium bromide

: 59961-15-8
methyl 3-(bromomethyl)thiophene-2-carboxylate

: 1243142-03-1
methyl 3-methylene [(2,4-dimethyl-phenyl)-phosphinate ethyl ester]thiophene-2-carboxylate

Guidance literature:: diethyl phosphorylchloridite; (2,4-dimethylphenyl)magnesium bromide; In tetrahydrofuran; at 20 ℃; for 1.75h; Inert atmosphere; Reflux;

methyl 3-(bromomethyl)thiophene-2-carboxylate; In tetrahydrofuran; Reflux;