(1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene

Base Information

Chemical Name:(1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene
CAS No.:194095-71-1
Molecular Formula:C₁₅H₁₇Cl
Molecular Weight:232.753
Hs Code.:

Synonyms:(1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene

Chemical Property:

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Technology Process of (1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene

There total 4 articles about (1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 194095-66-4
(3E,5E)-6-chloro-1-(p-isopropylphenyl)hexa-3,5-diene

: 194095-71-1
(1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene

Guidance literature:: With methanesulfonyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; Yield given; Multistep reaction; 1.) CH₂Cl₂, room temperature, 30 min, 2.) CH₂Cl₂, room temperature;
DOI:10.1016/S0040-4020(99)00123-4

Reference yield:

: 194095-62-0
(5E)-6-chloro-1-(p-isopropylphenyl)hex-5-en-3-yn-1-ol

: 194095-71-1
(1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Red-Al / diethyl ether; toluene / 5 h / -20 - 36 °C

2: 1.) methanesulfonyl chloride, triethylamine, 2.) DBU / 1.) CH₂Cl₂, room temperature, 30 min, 2.) CH₂Cl₂, room temperature

With methanesulfonyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; toluene;
DOI:10.1016/S0040-4020(99)00123-4

Reference yield:

: Methanesulfonic acid (3E,5E)-6-chloro-1-(4-isopropyl-phenyl)-hexa-3,5-dienyl ester

: 194095-71-1
(1E,3E,5E)-1-chloro-6-(p-isopropylphenyl)-1,3,5-hexatriene

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; Yield given; 0 deg C to room t.;
DOI:10.1016/S0040-4039(97)01156-8