{[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid

Base Information

• Chemical Name: {[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid
• CAS No.: 756798-74-0
• Molecular Formula: C₂₀H₂₁NO₇
• Molecular Weight: 387.389

Synonyms:{[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid

Chemical Property of {[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid

Chemical Property:

Purity/Quality:

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Technology Process of {[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid

There total 3 articles about {[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(3,5-dimethoxyphenyl)-2-hydroxy-1-phenylethan-1-one (34904-92-2) → {[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid (756798-74-0)

Guidance literature:

Multi-step reaction with 3 steps

1: DMAP / tetrahydrofuran / 3 h / Ambient temperature

2: 497 mg / NMM / tetrahydrofuran / 20 h / Ambient temperature

3: NaOH / methanol; H₂O / 3 h

With 4-methyl-morpholine; dmap; sodium hydroxide; In tetrahydrofuran; methanol; water;

DOI:10.1016/S0040-4020(97)00009-4

Reference yield:

Carbonic acid 1-(3,5-dimethoxy-phenyl)-2-oxo-2-phenyl-ethyl ester 4-nitro-phenyl ester (169309-14-2) → {[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid (756798-74-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 497 mg / NMM / tetrahydrofuran / 20 h / Ambient temperature

2: NaOH / methanol; H₂O / 3 h

With 4-methyl-morpholine; sodium hydroxide; In tetrahydrofuran; methanol; water;

DOI:10.1016/S0040-4020(97)00009-4

Reference yield:

{[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid ethyl ester → {[1-(3,5-Dimethoxy-phenyl)-2-oxo-2-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid (756798-74-0) + {[2-(3,5-Dimethoxy-phenyl)-2-oxo-1-phenyl-ethoxycarbonyl]-methyl-amino}-acetic acid

Guidance literature:

With sodium hydroxide; In methanol; water; for 3h;

DOI:10.1016/S0040-4020(97)00009-4

upstream raw materials:

2-(3,5-dimethoxyphenyl)-2-hydroxy-1-phenylethan-1-one

Carbonic acid 1-(3,5-dimethoxy-phenyl)-2-oxo-2-phenyl-ethyl ester 4-nitro-phenyl ester

Downstream raw materials:

5,7-Dimethoxy-2-phenylbenzofuran

sarcosine

carbon dioxide

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