(4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one

Base Information

Chemical Name:(4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one
CAS No.:717137-46-7
Molecular Formula:C₃₄H₃₄N₂O₃
Molecular Weight:518.656
Hs Code.:

Synonyms:(4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one

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Chemical Property of (4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one

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Technology Process of (4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one

There total 6 articles about (4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 170969-90-1
(3R,αS)-3-N-benzyl-N-α-methylbenzylamino-3-phenylpropanoic acid

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 717137-46-7
(4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one

Guidance literature:: (3R,αS)-3-N-benzyl-N-α-methylbenzylamino-3-phenylpropanoic acid; With pivaloyl chloride; triethylamine; In tetrahydrofuran; at -30 ℃; for 2h;

(S)-4-Benzyl-2-oxazolidinone; With lithium chloride; In tetrahydrofuran; at -30 - 20 ℃; for 12h;
DOI:10.1016/j.tetasy.2010.03.033

Reference yield: 84.0%

: 128891-66-7
(4S)-4-benzyl-3-[(2E)-3-phenylprop-2-enoyl]-1,3-oxazolidin-2-one

: lithium N-benzyl-N-((S)-1-phenylethyl)amide

: 717137-46-7
(4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one

Guidance literature:: DOI:10.1039/b401293c

Reference yield: 35.0%

: 17480-69-2
(S)-N-benzyl-1-phenylethylamine

: 14990-09-1
tert-butyl cinnamate

: 133812-18-7
(S)-4-benzyl-3-(6-(benzyloxy)hex-2-enoyl)oxazolidin-2-one

: 717137-46-7
(4S,3'R,αS)-3-{3'-[N-benzyl-N-(α-methylbenzyl)amino]-3'-phenylpropanoyl}-4-benzyloxazolidin-2-one

: tert-butyl (2S,3R,1'R,4''S,αS)-2-[1'-phenyl-1'(N-benzyl-N-α-methylbenzylamino)methyl]-3-phenyl-5-oxo-5-(4''-benzyl-oxazolidin-2''-one-3''-yl)pentanoate

: 265669-72-5
tert-butyl (3R,αS)-3-[N-benzyl-N-(α-methylbenzyl)amino]-3-phenylpropanoate

Guidance literature:: (S)-N-benzyl-1-phenylethylamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

tert-butyl cinnamate; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

(S)-4-benzyl-3-(6-(benzyloxy)hex-2-enoyl)oxazolidin-2-one; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 2h; Further stages.;
DOI:10.1039/b701226h