1,11-bis(trimethylsilyl)-3,9-dimethoxy-3,6,9-tris(4-methoxyphenyl)undeca-1,4,7,10-tetrayn-6-ol

Base Information

Chemical Name:1,11-bis(trimethylsilyl)-3,9-dimethoxy-3,6,9-tris(4-methoxyphenyl)undeca-1,4,7,10-tetrayn-6-ol
CAS No.:801287-42-3
Molecular Formula:C₄₀H₄₆O₆Si₂
Molecular Weight:678.973
Hs Code.:

Synonyms:1,11-bis(trimethylsilyl)-3,9-dimethoxy-3,6,9-tris(4-methoxyphenyl)undeca-1,4,7,10-tetrayn-6-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,11-bis(trimethylsilyl)-3,9-dimethoxy-3,6,9-tris(4-methoxyphenyl)undeca-1,4,7,10-tetrayn-6-ol

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Technology Process of 1,11-bis(trimethylsilyl)-3,9-dimethoxy-3,6,9-tris(4-methoxyphenyl)undeca-1,4,7,10-tetrayn-6-ol

There total 1 articles about 1,11-bis(trimethylsilyl)-3,9-dimethoxy-3,6,9-tris(4-methoxyphenyl)undeca-1,4,7,10-tetrayn-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 100-07-2
4-methoxy-benzoyl chloride

: 801287-33-2
1-trimethylsilyl-3-(4-methoxyphenyl)-3-methoxypenta-1,4-diyne

: 801287-42-3
1,11-bis(trimethylsilyl)-3,9-dimethoxy-3,6,9-tris(4-methoxyphenyl)undeca-1,4,7,10-tetrayn-6-ol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2004.07.052

Reference yield:

: 74-88-4
methyl iodide

: 801287-42-3
1,11-bis(trimethylsilyl)-3,9-dimethoxy-3,6,9-tris(4-methoxyphenyl)undeca-1,4,7,10-tetrayn-6-ol

: 801287-50-3
C₄₀H₄₆Si₂O₆CH₂

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; dimethyl sulfoxide; at -20 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2004.07.052