(S)-2-(DIBENZYLAMINO)-4-METHYL-1-PENTANOL

Base Information

Chemical Name:(S)-2-(DIBENZYLAMINO)-4-METHYL-1-PENTANOL
CAS No.:307532-07-6
Molecular Formula:C20H27 N O
Molecular Weight:297.44
Hs Code.:2922199090
Mol file:307532-07-6.mol

Synonyms:N,N-DIBENZYL-L-LEUCINOL;(S)-2-(DIBENZYLAMINO)-4-METHYL-1-PENTANOL;(S)-(+)-2-(N,N-DIBENZYLAMINO)-4-METHYLPENTANOL

Suppliers and Price of (S)-2-(DIBENZYLAMINO)-4-METHYL-1-PENTANOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N,N-DIBENZYL-D-LEUCINOL 95.00%
5MG
$ 497.21

Total 9 raw suppliers

Chemical Property of (S)-2-(DIBENZYLAMINO)-4-METHYL-1-PENTANOL

Chemical Property:

PSA：23.47000
LogP:4.09580

Purity/Quality:

98% ^*data from raw suppliers

N,N-DIBENZYL-D-LEUCINOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of (S)-2-(DIBENZYLAMINO)-4-METHYL-1-PENTANOL

There total 2 articles about (S)-2-(DIBENZYLAMINO)-4-METHYL-1-PENTANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 7533-40-6,16369-17-8,53448-09-2,502-32-9,14438-11-0
2-amino-4-methyl-1-pentanol

: 100-39-0
benzyl bromide

: 307532-07-6
(2R)-2-(dibenzylamino)-4-methylpentan-1-ol

Guidance literature:: With potassium carbonate; In ethanol; at 20 ℃; for 96h;
DOI:10.1016/j.bmc.2013.06.057

Reference yield:

: 691-37-2,25068-26-2
4-Methyl-1-pentene

: 52742-32-2
N,N-dibenzyl-O-benzoylhydroxylamine

: C₁₆H₈B₂O₄

: 111060-53-8
(S)-2-(N,N-dibenzylamino)-4-methyl-1-pentanol

: 307532-07-6
(2R)-2-(dibenzylamino)-4-methylpentan-1-ol

Guidance literature:: 4-Methyl-1-pentene; N,N-dibenzyl-O-benzoylhydroxylamine; C₁₆H₈B₂O₄; With (R,R)-PTBP-Skewphos; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; ethanol; water; at 20 ℃; for 0.5h; Overall yield = 30 %; Overall yield = 22 mg; enantioselective reaction;
DOI:10.1002/chem.201801070