tert-butyl 2-(4-tert-butylcyclohexylidene)hydrazinecarboxylate

Base Information

• Chemical Name: tert-butyl 2-(4-tert-butylcyclohexylidene)hydrazinecarboxylate
• CAS No.: 60295-14-9
• Molecular Formula: C15H28 N2 O2
• Molecular Weight: 268.395
• Mol file: 60295-14-9.mol

Synonyms:Hydrazinecarboxylicacid, [4-(1,1-dimethylethyl)cyclohexylidene]-, 1,1-dimethylethyl ester (9CI);NSC 148513

Chemical Property of tert-butyl 2-(4-tert-butylcyclohexylidene)hydrazinecarboxylate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.01g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl 2-(4-tert-butylcyclohexylidene)hydrazinecarboxylate

There total 2 articles about tert-butyl 2-(4-tert-butylcyclohexylidene)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(tert-butyloxycarbonyl) azide (1070-19-5) + 4-tercbutyl-cyclohexanone (98-53-3) → N'-(4-tert-butyl-cyclohexylidene)-hydrazinecarboxylic acid tert-butyl ester (60295-14-9)

Guidance literature:

In ethanol;

DOI:10.1021/jo00886a007

Reference yield:

t-butoxycarbonylhydrazine (870-46-2) + 4-tercbutyl-cyclohexanone (98-53-3) → N'-(4-tert-butyl-cyclohexylidene)-hydrazinecarboxylic acid tert-butyl ester (60295-14-9)

Guidance literature:

In dichloromethane; for 18h; Presence of drying agents;

Reference yield:

N'-(4-tert-butyl-cyclohexylidene)-hydrazinecarboxylic acid tert-butyl ester (60295-14-9) → N'-(4-tert-butyl-cyclohexyl)-hydrazinecarboxylic acid tert-butyl ester (60295-42-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1021/jo00886a007

upstream raw materials:

N-(tert-butyloxycarbonyl) azide

4-tercbutyl-cyclohexanone

t-butoxycarbonylhydrazine

Downstream raw materials:

N'-(4-tert-butyl-cyclohexyl)-hydrazinecarboxylic acid tert-butyl ester

C₁₀H₂₂N₂

(E)-3-{4-[1-(4-tert-butylcyclohexyl)-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-ylazo]-3-hydroxyphenyl}-2-methylacrylic acid

Refernces