3β-O-benzylchlorogenin

Base Information

Chemical Name:3β-O-benzylchlorogenin
CAS No.:210687-05-1
Molecular Formula:C₃₄H₅₀O₄
Molecular Weight:522.769
Hs Code.:

Synonyms:3β-O-benzylchlorogenin

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Chemical Property of 3β-O-benzylchlorogenin

Chemical Property:

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Technology Process of 3β-O-benzylchlorogenin

There total 6 articles about 3β-O-benzylchlorogenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 146333-24-6
3-O-benzyl diosgenin

: 210687-05-1
3β-O-benzylchlorogenin

Guidance literature:: 3-O-benzyl diosgenin; With diborane-dimethylsulfide complex; In tetrahydrofuran; at 20 ℃;

With sodium hydroxide; dihydrogen peroxide; at 20 ℃;
DOI:10.1016/j.carres.2005.03.019

Reference yield:

: 512-04-9
diosgenin

: 210687-05-1
3β-O-benzylchlorogenin

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / NaH / tetrahydrofuran; dimethylformamide / Heating

2.1: B₂H₆*MeS₂ / tetrahydrofuran / 20 °C

2.2: 71 percent / aq. NaOH; aq. H₂O₂ / 20 °C

With diborane-dimethylsulfide complex; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2005.03.019

Reference yield:

: 100-39-0
benzyl bromide

: 210687-05-1
3β-O-benzylchlorogenin

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaH, tetrabutylammonium iodide / tetrahydrofuran / 16 h / Heating

2: 1.) BH₃-SMe₂, 2.) H₂O₂, NaOH / 1.) THF, 0 deg C, 0.1 h, room temperature, 20 h, 2.) ethanol, water, reflux, 1 h

With sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo980266c