Benzoic acid (Z)-(R)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester

Base Information

• Chemical Name: Benzoic acid (Z)-(R)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester
• CAS No.: 107613-13-8
• Molecular Formula: C₂₇H₃₆O₆
• Molecular Weight: 456.579

Synonyms:Benzoic acid (Z)-(R)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester

Chemical Property of Benzoic acid (Z)-(R)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester

Chemical Property:

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Technology Process of Benzoic acid (Z)-(R)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester

There total 1 articles about Benzoic acid (Z)-(R)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-(4S,5S,6S)-6-Benzyloxy-5-(2-methoxy-ethoxymethoxy)-3,5-dimethyl-hept-2-en-4-ol (107657-73-8) + benzoyl chloride (98-88-4) → Benzoic acid (Z)-(S)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester (107613-13-8,110549-64-9)

Guidance literature:

DOI:10.1016/S0040-4039(00)84485-8

Reference yield: 41.0%

Benzoic acid (Z)-(R)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester (107613-13-8) → Benzoic acid (2R,3S,4R,5S)-2-(1-iodo-ethyl)-4-(2-methoxy-ethoxymethoxy)-2,4,5-trimethyl-tetrahydro-furan-3-yl ester (98095-65-9) + (+/-)-(2R*,3S*,4S*,5R*)-4-<(2-methoxyethoxy)methoxy>-2-(1-iodoethyl)-2,4,5-trimethyl-3-tetrahydrofuranyl benzoate (98095-65-9,107657-76-1,107657-77-2,110549-58-1,110549-59-2)

Guidance literature:

With iodine; sodium hydrogencarbonate; In acetonitrile; at 0 ℃; for 3h;

DOI:10.1021/jo00232a001

Reference yield:

Benzoic acid (Z)-(S)-1-[(1R,2S)-2-benzyloxy-1-(2-methoxy-ethoxymethoxy)-1-methyl-propyl]-2-methyl-but-2-enyl ester (107613-13-8,110549-64-9) → Benzoic acid (2R,3R,4R,5S)-2-((S)-1-iodo-ethyl)-4-(2-methoxy-ethoxymethoxy)-2,4,5-trimethyl-tetrahydro-furan-3-yl ester (98095-65-9,107657-76-1,107657-77-2,110549-58-1,110549-59-2)

Guidance literature:

With iodine; sodium hydrogencarbonate; In acetonitrile; at 0 ℃;

DOI:10.1016/S0040-4039(00)84485-8

upstream raw materials:

(Z)-(4S,5S,6S)-6-Benzyloxy-5-(2-methoxy-ethoxymethoxy)-3,5-dimethyl-hept-2-en-4-ol

benzoyl chloride

Downstream raw materials:

(+/-)-(2S^*,3S^*,4R^*,5R^*)-4-<(2-methoxyethoxy)methoxy>-2,4,5-trimethyl-2-vinyl-3-tetrahydrofuranol

(+/-)-(2R^*,3S^*,4S^*,5R^*)-4-<(2-methoxyethoxy)methoxy>-2,4,5-trimethyl-2-vinyl-3-tetrahydrofuranyl benzoate

Benzoic acid (2R,3S,4R,5S)-2-(1-iodo-ethyl)-4-(2-methoxy-ethoxymethoxy)-2,4,5-trimethyl-tetrahydro-furan-3-yl ester

(+/-)-(2R^*,3S^*,4S^*,5R^*)-4-<(2-methoxyethoxy)methoxy>-2-(1-iodoethyl)-2,4,5-trimethyl-3-tetrahydrofuranyl benzoate

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