but-2-yn-1-yl 3-phenylpropiolate

Base Information

Chemical Name:but-2-yn-1-yl 3-phenylpropiolate
CAS No.:1253101-11-9
Molecular Formula:C₁₃H₁₀O₂
Molecular Weight:198.221
Hs Code.:

Synonyms:but-2-yn-1-yl 3-phenylpropiolate

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Chemical Property of but-2-yn-1-yl 3-phenylpropiolate

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Technology Process of but-2-yn-1-yl 3-phenylpropiolate

There total 4 articles about but-2-yn-1-yl 3-phenylpropiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 764-01-2
methyl propargyl alcohol

: 637-44-5
phenylpropyolic acid

: 1253101-11-9
but-2-yn-1-yl 3-phenylpropiolate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃;
DOI:10.1055/s-0034-1380524

Reference yield: 83.0%

: 124-38-9,18923-20-1
carbon dioxide

: 3355-17-7
1-chloro-2-butyne

: 536-74-3
phenylacetylene

: 1253101-11-9
but-2-yn-1-yl 3-phenylpropiolate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 24h; under 3750.38 Torr; Autoclave;
DOI:10.1002/cctc.201900039

Reference yield: 42.0%

: 124-38-9,18923-20-1
carbon dioxide

: 3355-28-0
1-Bromo-2-butyne

: 536-74-3
phenylacetylene

: 1253101-11-9
but-2-yn-1-yl 3-phenylpropiolate

Guidance literature:: With caesium carbonate; silver(I) iodide; In acetonitrile; at 40 ℃; for 48h; under 760.051 Torr; Schlenk technique;
DOI:10.1016/j.tet.2016.12.075