4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane

Base Information

• Chemical Name: 4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane
• CAS No.: 1384099-55-1
• Molecular Formula: C₂₁H₂₄F₃N₃
• Molecular Weight: 375.437

Synonyms:4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane

Chemical Property of 4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane

Chemical Property:

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Technology Process of 4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane

There total 2 articles about 4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane (1384099-49-3) + benzyl bromide (100-39-0) → 4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane (1384099-55-1)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 4h;

DOI:10.1016/j.tet.2012.04.057

Reference yield:

4-Trifluoromethylbenzaldehyde (455-19-6) → 4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane (1384099-55-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 4 h / 20 °C / Molecular sieve

2: potassium carbonate / acetonitrile / 4 h / 20 °C

With potassium carbonate; In ethanol; acetonitrile;

DOI:10.1016/j.tet.2012.04.057

Reference yield: 100.0%

4-benzyl-10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane (1384099-55-1) → 1-benzyl-1,4,7-triazacyclononane trihydrochloride

Guidance literature:

With hydrogenchloride; water; at 20 ℃; for 3h;

DOI:10.1016/j.tet.2012.04.057

upstream raw materials:

4-Trifluoromethylbenzaldehyde

10-(4-(trifluoromethyl)phenyl)-1,4,7-triazabicyclo[5.2.1]decane

benzyl bromide

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