4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole

Base Information

• Chemical Name: 4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole
• CAS No.: 124512-17-0
• Molecular Formula: C₂₄H₂₂N₄O₂S
• Molecular Weight: 430.53

Synonyms:4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole

Chemical Property of 4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole

Chemical Property:

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Technology Process of 4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole

There total 2 articles about 4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

i-propyl isocyanide (598-45-8) + 1-Benzhydrylidene-3-(4-nitro-phenyl)-thiourea (124512-04-5) → 4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole (124512-17-0)

Guidance literature:

In tetrahydrofuran; for 22h; Heating;

DOI:10.1021/jo00293a011

Reference yield:

Benzophenone imine (1013-88-3) → 4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole (124512-17-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran / 72 h / Ambient temperature

2: 84 percent / tetrahydrofuran / 22 h / Heating

In tetrahydrofuran;

DOI:10.1021/jo00293a011

Reference yield: 72.0%

4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole (124512-17-0) → 5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine (128569-64-2)

Guidance literature:

With 2,6-dichloro-benzonitrile; In acetonitrile; for 3h; Heating;

DOI:10.1021/jo00293a011

upstream raw materials:

i-propyl isocyanide

1-Benzhydrylidene-3-(4-nitro-phenyl)-thiourea

Benzophenone imine

Downstream raw materials:

5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine

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