3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate

Base Information

Chemical Name:3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate
CAS No.:1595291-52-3
Molecular Formula:C₁₅H₂₂BNO₄
Molecular Weight:291.155
Hs Code.:

Synonyms:3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate

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Chemical Property of 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate

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Technology Process of 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate

There total 7 articles about 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 214360-76-6
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 1595291-52-3
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 71.0%

: 16088-19-0
norneostigmine

: 73183-34-3
bis(pinacol)diborane

: 1595291-52-3
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate

Guidance literature:: With air; In 1,4-dioxane; at 20 ℃; for 48h; Irradiation;
DOI:10.1021/acs.orglett.1c03590

Reference yield: 66.0%

: 3-(pyridin-2-yloxy)phenyl dimethylcarbamate

: 73183-34-3
bis(pinacol)diborane

: 1595291-52-3
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl dimethylcarbamate

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tricyclohexylphosphine; In toluene; at 120 ℃; for 15h; Glovebox; Inert atmosphere;
DOI:10.1021/ja511622e