15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid

Base Information

Chemical Name:15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid
CAS No.:868836-26-4
Molecular Formula:C₄₆H₆₂N₄O₇S₂
Molecular Weight:847.153
Hs Code.:

15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid

Synonyms:15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid

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Chemical Property of 15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid

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Technology Process of 15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid

There total 6 articles about 15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.2%

: 868836-22-0
15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanoic acid

: 868836-26-4
15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid

Guidance literature:: 15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanoic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.333333h;

With hydroxylamine; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;
DOI:10.1021/jm0505009

Reference yield: 70.2%

: 868836-26-4
15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid

Guidance literature:

Reference yield:

: C₃₃H₄₁N₃O₆S₂

: 868836-26-4
15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-11-[N-2,4,6-(trimethyl)benzenesulfonyl]-6-oxo-7,11-diazapentadecanohydroxamic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylformamide / 0.5 h / 0 °C

1.2: 60.3 percent / dimethylformamide / 12 h

2.1: 78.5 percent / hydrazine / methanol / 12 h / Heating

3.1: 72.6 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

4.1: 80 percent / aq. LiOH / tetrahydrofuran / 0 - 20 °C

5.1: ethyl chloroformate; triethylamine / tetrahydrofuran / 0.33 h / 0 °C

5.2: 70.2 percent / hydroxylamine / methanol; tetrahydrofuran / 0.5 h / 20 °C

With lithium hydroxide; chloroformic acid ethyl ester; sodium hydride; triethylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0505009