5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline

Base Information

Chemical Name:5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline
CAS No.:528584-33-0
Molecular Formula:C₁₉H₁₄Cl₂N₄O₂S
Molecular Weight:433.318
Hs Code.:

Synonyms:5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline

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Chemical Property of 5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline

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Technology Process of 5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline

There total 3 articles about 5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 79-04-9
chloroacetyl chloride

: 528583-97-3
5-(4-acetylphenylazo)-2-amino-4-(2-chlorophenyl)thiazole

: 528584-33-0
5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline

Guidance literature:: With triethylamine; In benzene; at 20 ℃; for 2h;
DOI:10.1002/jhet.5570390604

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 528584-33-0
5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / iodine / 12 h / Heating

2: 95 percent / aq. sodium nitrite; HCl; sodium acetate / aq. ethanol / 2 h / -5 °C

3: 88 percent / triethylamine / benzene / 2 h / 20 °C

With hydrogenchloride; iodine; sodium acetate; triethylamine; sodium nitrite; In ethanol; benzene;
DOI:10.1002/jhet.5570390604

Reference yield:

: 21344-90-1
4-(o-chlorophenyl)-1,3-thiazol-2-amine

: 528584-33-0
5-(4-acetylphenylazo)-3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-iminothiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / aq. sodium nitrite; HCl; sodium acetate / aq. ethanol / 2 h / -5 °C

2: 88 percent / triethylamine / benzene / 2 h / 20 °C

With hydrogenchloride; sodium acetate; triethylamine; sodium nitrite; In ethanol; benzene;
DOI:10.1002/jhet.5570390604