1,3-dibenzyl-5-phenylpyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:1,3-dibenzyl-5-phenylpyrimidine-2,4(1H,3H)-dione
CAS No.:1309609-19-5
Molecular Formula:C₂₄H₂₀N₂O₂
Molecular Weight:368.435
Hs Code.:

Synonyms:1,3-dibenzyl-5-phenylpyrimidine-2,4(1H,3H)-dione

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Chemical Property of 1,3-dibenzyl-5-phenylpyrimidine-2,4(1H,3H)-dione

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,3-dibenzyl-5-phenylpyrimidine-2,4(1H,3H)-dione

There total 2 articles about 1,3-dibenzyl-5-phenylpyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 591-50-4
iodobenzene

: 34001-56-4
1,3-dibenzyluracil

: 1309609-19-5
1,3-dibenzyl-5-phenylpyrimidine-2,4(1H,3H)-dione

: 1,3-dibenzyl-6-phenylpyrimidine-2,4(1H,3H)-dione

Guidance literature:: With palladium diacetate; caesium carbonate; tris(pentafluorophenyl)phosphine; In N,N-dimethyl-formamide; at 160 ℃; for 48h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo2006494

Reference yield:

: 100-39-0
benzyl bromide

: 1309609-19-5
1,3-dibenzyl-5-phenylpyrimidine-2,4(1H,3H)-dione

: 1,3-dibenzyl-6-phenylpyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / Inert atmosphere

1.2: 72 h / Inert atmosphere

2.1: copper(l) iodide; palladium diacetate; caesium carbonate; tris(pentafluorophenyl)phosphine / N,N-dimethyl-formamide / 48 h / 160 °C / Inert atmosphere

With copper(l) iodide; palladium diacetate; potassium carbonate; caesium carbonate; tris(pentafluorophenyl)phosphine; In N,N-dimethyl-formamide;
DOI:10.1021/jo2006494