(E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone

Base Information

Chemical Name:(E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone
CAS No.:210166-25-9
Molecular Formula:C₃₆H₂₉IO₅
Molecular Weight:668.528
Hs Code.:

Synonyms:(E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone

Chemical Property:

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Technology Process of (E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone

There total 4 articles about (E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-3-iodo-2-methoxymethoxy-phenyl)-propenone

: 210166-25-9
(E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone

Guidance literature:: With hydrogenchloride; In ethanol; chloroform; at 40 ℃; for 1h; Yield given;

Reference yield:

: 18065-05-9
1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone

: 210166-25-9
(E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / silver trifluoroacetate, I₂ / CHCl₃ / 0.5 h / Ambient temperature

2: 90 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 1.25 h / Ambient temperature

3: KOH / ethanol / 4.5 h / Heating

4: conc. aq. HCl / CHCl₃; ethanol / 1 h / 40 °C

With hydrogenchloride; potassium hydroxide; iodine; silver trifluoroacetate; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; chloroform;

Reference yield:

: 95165-66-5
3-Iod-2-hydroxy-4,6-dibenzyloxy-acetophenon

: 210166-25-9
(E)-3-(4-Benzyloxy-phenyl)-1-(4,6-bis-benzyloxy-2-hydroxy-3-iodo-phenyl)-propenone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 1.25 h / Ambient temperature

2: KOH / ethanol / 4.5 h / Heating

3: conc. aq. HCl / CHCl₃; ethanol / 1 h / 40 °C

With hydrogenchloride; potassium hydroxide; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; chloroform;