(+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

Base Information

Chemical Name:(+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine
CAS No.:78167-91-6
Molecular Formula:C₂₁H₁₉NO₄
Molecular Weight:349.386
Hs Code.:

(+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenz<c>acridine

Synonyms:(+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

Suppliers and Price of (+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

There total 1 articles about (+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 563-63-3
silver(I) acetate

: 54538-09-9
1,2,3,4-Tetrahydrobenzacridine

: 225-51-4,208851-55-2
benz[c]acridine

: 78167-94-9
(+/-)-trans-1,2-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

: 78167-91-6
(+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); iodine; lithium carbonate; lithium fluoride; Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1021/jo00331a019

Reference yield:

: 78167-91-6
(+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

: 78167-93-8,77305-76-1
3,4-dihydro-3,4-dihydroxybenzacridine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NBS, AIBN / CCl₄ / 30 h / 70 - 75 °C

2: 82 percent / Li₂CO₃, LiF / hexamethylphosphoric acid triamide / 6 h / 90 - 95 °C

3: 85 percent / NH₃(gas)/MeOH / methanol; tetrahydrofuran / 2 h / Ambient temperature

With methanol; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonia; lithium carbonate; lithium fluoride; In tetrahydrofuran; methanol; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/jo00331a019

Reference yield:

: 78167-91-6
(+/-)-trans-3,4-Diacetoxy-1,2,3,4-tetrahydrobenzacridine

: 78167-99-4,82009-66-3
(+/-)-3α,4β-Dihydroxy-1α,2α-epoxy-1,2,3,4-tetrahydrobenzacridine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / NBS, AIBN / CCl₄ / 30 h / 70 - 75 °C

2: 82 percent / Li₂CO₃, LiF / hexamethylphosphoric acid triamide / 6 h / 90 - 95 °C

3: 85 percent / NH₃(gas)/MeOH / methanol; tetrahydrofuran / 2 h / Ambient temperature

4: 72 percent / m-CPBA / tetrahydrofuran / 1 h / Ambient temperature

With methanol; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonia; lithium carbonate; lithium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/jo00331a019