5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione

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Chemical Name:5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione
CAS No.:287933-85-1
Molecular Formula:C₁₇H₁₈N₂O₆
Molecular Weight:346.34
Hs Code.:

Synonyms:5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione

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Chemical Property of 5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione

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Technology Process of 5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione

There total 12 articles about 5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 98-88-4
benzoyl chloride

: 448896-39-7
5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-hydroxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione

: 287933-85-1
5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione

Guidance literature:: With pyridine; at -20 - -10 ℃; for 1h;
DOI:10.1016/S0040-4039(00)00467-6

Reference yield:

: 287933-84-0
5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

: 287933-85-1
5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Amberlyst 15-H / methanol / 12 h / 20 °C

2: 95 percent / CH₂Cl₂; pyridine / 2 h / -40 - -5 °C

With Amberlyst 15-H; In pyridine; methanol; dichloromethane;
DOI:10.1007/s007060200024

Reference yield:

: 287933-97-5
2,2'-anhydro-5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-(((4-methoxyphenyl)-diphenylmethoxy)-methyl)-1-furanyl)-2,4(1H,3H)-pyrimidinedione

: 287933-85-1
5-methyl-1-((1R,2S,3S)-tetrahydro-2-hydroxy-3-benzoyloxymethyl-1-furanyl)-2,4(1H,3H)-pyrimidinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / aq. NaOH / ethanol / 9 h / 20 °C

2: 100 percent / Amberlyst 15-H / methanol / 12 h / 20 °C

3: 95 percent / CH₂Cl₂; pyridine / 2 h / -40 - -5 °C

With sodium hydroxide; Amberlyst 15-H; In pyridine; methanol; ethanol; dichloromethane;
DOI:10.1007/s007060200024