5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride

Base Information

Chemical Name:5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride
CAS No.:127382-95-0
Molecular Formula:C₁₆H₁₇N₃O₄*ClH
Molecular Weight:351.79
Hs Code.:

Synonyms:5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride

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Chemical Property of 5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride

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Technology Process of 5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride

There total 4 articles about 5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 39828-35-8
2,4-dimethoxybenzoyl chloride

: 127356-17-6
5-acetyl-2,3-diaminopyridine

: 127382-95-0
5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride

Guidance literature:: With pyridine; triethylamine; In acetone; for 3h;
DOI:10.1021/jm00170a030

Reference yield:

: 127356-41-6
5-acetyl-2-amino-3-nitropyridine

: 127382-95-0
5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / H₂ / 10percent Pd/C / methanol

2: 64 percent / Et₃N, pyridine / acetone / 3 h

With pyridine; hydrogen; triethylamine; palladium on activated charcoal; In methanol; acetone;
DOI:10.1021/jm00170a030

Reference yield:

: 23945-84-8
6-chloro-5-nitro-nicotinoyl chloride

: 127382-95-0
5-acetyl-2-amino-3-<(2,4-dimethoxybenzoyl)amino>pyridine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

2: 83 percent / aq. NH₃ / ethanol / 3 h / Ambient temperature

3: 39 percent / H₂ / 10percent Pd/C / methanol

4: 64 percent / Et₃N, pyridine / acetone / 3 h

With pyridine; ammonium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; acetone;
DOI:10.1021/jm00170a030