MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)

Base Information

Chemical Name:MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)
CAS No.:916042-47-2
Molecular Formula:C₈₆H₁₁₉ClMoN₄O₂
Molecular Weight:1372.31
Hs Code.:

MoCl(C<sub>6</sub>H<sub>3</sub>(OCH<sub>3</sub>)2NCH<sub>2</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>2</sub>(CH(CH<sub>3</sub>)2)3)2)2)

Synonyms:MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)

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Chemical Property of MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)

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Technology Process of MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)

There total 1 articles about MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 16998-75-7
tetrachlorobis(tetrahydrofurano)molybdenum(IV)

: 916042-40-5
C₆H₃(OCH₃)2NHCH₂CH₂N(CH₂CH₂NHC₆H₃(C₆H₂(CH(CH₃)2)3)2)2

: 916042-47-2
MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; under N2 atm. soln. MoCl4(THF)2 and ligand in THF was stirred for 1 h, (Me3Si)2NLi was added slowly and stirred for 2 h; solvent was removed in vacuo, residue was extd. with pentane, passed through Celite and evapd. to dryness in vacuo, recrystn. from pentane; elem. anal.;
DOI:10.1021/ic0613457

Reference yield: 75.0%

: 916042-47-2
MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)

: 7664-41-7
ammonia

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 916042-75-6
Mo(NH₃)(C₆H₃(OCH₃)2NC₂H₄N(C₂H₄NC₃₆H₄₉)2)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=(Mo(NH₃)(C₆H₃(OCH₃)2NC₂H₄N(NC₃₈H₅₃)2))B(C₆H₃(CF₃)2)4

Guidance literature:: In dichloromethane; Mo complex, NaBAr4, and NH3 in CH2Cl2 in Teflon-sealed vessel were stirred for 6 h; voilatiles were removed in vacuo, residue was extd. with pentane, filtered through Celite, solvent was removed in vacuo, residue was recrystd. from pentane; elem. anal.;
DOI:10.1021/ic0613457

Reference yield: 55.0%

: 916042-47-2
MoCl(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)

: 4648-54-8
trimethylsilylazide

: MoN(C₆H₃(OCH₃)2NCH₂CH₂N(CH₂CH₂NC₆H₃(C₆H₂(CH(CH₃)2)3)2)2)

Guidance literature:: In benzene; High Pressure; under N2 atm. Me3SiN3 and Mo complex in benzene in Teflon-sealed glass bomb were heated at 100°C overnight; solvent was stripped to dryness in vacuo, residue was taken in pentane, filtered through Celite, evapd. in vacuo, and recrystd. from pentane; elem. anal.;
DOI:10.1021/ic0613457